反应条件
in neat (no solvent) byproducts: Me3SiF, (CF3S)2; (Me3Si)2NSCF3 and BBr3 were condensed into a vessel, and stirred at 50 °C for 72 h; further, not identified products;; sepn. by fractionated condensation at -30, -80, and -196°C, not isolated, identified by IR, MS, and 19F NMR, quantified by (11)B NMR;;
参考文献
Haas, Alois; Willert-Porada, Monika
Chemische Berichte, 1985 , vol. 118, # 4 p. 1463 - 1475