byproducts: HCl; 450°C, sealed tube; cooling to room temp. over 12 h yields crystals, evapn. of volatile products, boraadamantane is sublimated in vac., elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 367, p. 19 - 26
in chloroform-d1 under N2, with exclusion of moisture, condensed reagents (1/1 or 1.14/0.55 mmol ratio) gently warmed to room temp.; not sepd.; detected by NMR, IR;
