in benzene (N2); liquid BCl3 (46.0 mmol) condensed into soln. of the phenylene; mixt. allowed to warm to ambient temp.; 3 h stirring; (N2); solvent removed (vac.); residue distn. (50 °C, 1 mmHg);
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1689 - 1692
in diethyl ether; benzene by refluxing of phenyllithium is dissolved in benzene:ether=7:3;
参考文献
Reynard, K. E.; Sherman, R. E.; Smith, H. D.; Hohnstedt, L. F.
Inorganic Syntheses, 1973 , vol. 14, p. 52 - 55
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Gmelin Handbook: B: B-Verb.8, 11.2.4.1, page 173 - 175
