in neat (no solvent) heating of BCl3 and CFCl3 in an evacuated sealed tube at 65°C. for 283 h, then 4 h at 130°C; products detected by (11)B- and (19)F-NMR;
参考文献
Saulys, D. A; Castillo, J.; Morrison, J. A.
Inorganic Chemistry, 1989 , vol. 28, p. 1619 - 1624
in neat (no solvent) co-condensation of NMe3 and BCl3 in a glass bulb with slight excess of base at liquid nitrogen temp. in all-glass vacuum system; warming the mixture at ambient temp.; pumping excess of reactants off;;
参考文献
Sreekanth, C. S.; Mok, C. Y.; Huang, H. H.; Tan, K. L.
Journal of Electron Spectroscopy and Related Phenomena, 1992 , vol. 58, p. 129 - 140
