反应条件
in neat (no solvent) byproducts: Me3SiCl, Me3SiF; (Me3Si)2NSCF3 and BCl3 were condensed into a closed vessel and stirred at 50 °C for 72 h;; sepn. by fractionated condensation at -30, -80, and -196°C, not isolated, identified by IR and 19F NMR, quantified by 11B NMR;;
参考文献
Haas, Alois; Willert-Porada, Monika
Chemische Berichte, 1985 , vol. 118, # 4 p. 1463 - 1475
