反应条件
iron(III) chloride in neat (no solvent) FeCl3 loaded into reactor, evacuated, B compd. condensed at -196°C, sealed, warmed to 40°C for 4 d; distd., residue extd. with C6H6, C6H6 removed (vac.), sublimed at 45°C;
参考文献
Inorganic Chemistry, , vol. 21, p. 3662 - 3665
