反应条件
in pentane Ar-atmosphere; mixing BCl3, hexene and Et2SiH2 at -100°C, stirring for 1 h, addn. of MeOH, warming to room temp., stirring overnight; sepd. of pentane layer, collection (distillation, 152-170°C/700 Torr);
参考文献
Soundararajan, Raman; Matteson, Donald S.
Organometallics, 1995 , vol. 14, p. 4157 - 4166