Gerrard, W.; Mooney, E. F.; Rees, R. G.
Journal of the Chemical Society, 1964 , p. 740 - 745
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.3.4.5, page 87 - 88
in hexane; toluene under N2; soln. of BCl3 (1.05 equiv) in hexanes added dropwise to suspn.of (CuMes)5*toluene in toluene at -78 °C; mixt. stirred at -78 . degree.C for 2 h and then allowed to slowly warm to room temp. overnight; after filtration all volatiles removed under high vac.; crude product purified by distn. under reduced pressure; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 681, # 1-2 p. 134 - 142
n-butyllithium in diethyl ether 0°C, allowing to warm to room temp. after addn. of OHCH2CF3 and n-C4H9Li, stirring for 1 h, recooling to -78°C, addn. of BCl3, molar ratio of C6H5BCl2:OHCH2CF3:n-C4H9Li=1:3:3, stirring overnight;
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Shaw, S. Yvette; Neilson, Robert H.
Inorganic Chemistry, 1991 , vol. 30, p. 148 - 150
