tetrachloromethane in gas byproducts: HCl, Cl2, C6Cl6; vac. pyrolysis (340 and 420°C, varying molar ratio); fractional condensation, identification by MS and NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 361, p. C54 - C56
chlorine in neat (no solvent) addn. of mixt. of B-compds. to NMR tube contg. freshly sublimed AlCl3, addn. of Cl2 gas, warmed from -190°C to room temp., kept for 7 d; not isolated; detected by NMR;
