反应条件
in further solvent(s) byproducts: 1-butene; addn. of stannane to soln. of BCl3 (1.3 equiv. in 1,1,2,2-tetrachloroethane) at -40°C, stirring for 10 min at -40°C; trap-to-trap distn. (removing solvent at -50°C, distn. of productat -80°C); NMR spectroscopy (isomers not sepd., Z:E ratio 1:1);
参考文献
Le Serre, Stephanie; Guillemin, Jean-Claude
Organometallics, 1997 , vol. 16, # 26 p. 5844 - 5848
