反应条件
in n-heptane; dichloromethane (N2); indene dissolved in Et2O, MeLi/Et2O added with stirring at room temp., stirred for 40 min, a suspn. of ZrCl4 in pentane added, stirred at room temp. for 2 h, concd. (vac.), the powder slurried in CH2Cl2, BCl3 in heptane added at 0°C,; allowed to warm to room temp., stirred for 30 min, filtered, extd. with the same CH2Cl2 for 8 h, concd. (vac.); elem. anal.;
参考文献
Balboni, Davide; Camurati, Isabella; Ingurgio, Antonio Cascio; Guidotti, Simona; Focante, Francesca; Resconi, Luigi
Journal of Organometallic Chemistry, 2003 , vol. 683, # 1 p. 2 - 10
