NaH in tetrahydrofuran byproducts: H2; borane and THF condensing onto KH and Bu4NI under N2 at -196°C, warming to room temp., stirring for 15-18 h, THF removing, BBr3 condensing onto the residue at -196°C , warming to room temp., stirring for 6 h; isolated by sublimation; identified by NMR spectrum;
参考文献
Toft, Mark A.; Leach, J. B.; Himpsl, Francis L.; Shore, Sheldon G.
Inorganic Chemistry, 1982 , vol. 21, p. 1952 - 1957
NaH in tetrahydrofuran byproducts: H2, NaCl; borane and THF condensing onto NaH and Me4NCl under N2 at -196°C, warming to room temp., stirring for 12 h, THF removing, BCl3 condensing onto the residue at -196°C , warming to room temp., stirring for 6 h; isolated by sublimation; identified by NMR spectrum;
参考文献
Toft, Mark A.; Leach, J. B.; Himpsl, Francis L.; Shore, Sheldon G.
Inorganic Chemistry, 1982 , vol. 21, p. 1952 - 1957
