in dichloromethane
N2 atmosphere, condensation of BCl3 to soln. of stannyl compound at -50°C, warming to room temp., stirring (room temp., 17 h); removement of volatiles (25°C, 12 Torr), spectroscopic yield 100percent, MeBCl2/Me2BCl ratio 10:0.5, not isolated;
参考文献
Diemer, Stefan; Noeth, Heinrich; Storch, Wolfgang
European Journal of Inorganic Chemistry, 1999 , # 9 p. 1765 - 1780
Wiberg, E.; Ruschmann, W.
Ber., 1937 , vol. 70, p. 1583 - 1591
Full Text Show Details
Gmelin Handbook: B: SVol.1, 4.12, page 245 - 248
Full Text Show Details
Goubeau, J.
FIAT Review, Vol. 23, p. 226/38