Chambers,R.D.; Chivers,T.
Journal of the Chemical Society, 1965 , p. 3933 - 3939
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Gmelin Handbook: F: PerFHalOrg.4, 3.1.3.1, page 118 - 118
Chambers, R. D.; Cunningham, J. A.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 2185 - 2188
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Gmelin Handbook: F: PerFHalOrg.4, 3.1.3.1, page 118 - 118
in neat (no solvent)
byproducts: n-Bu3SnCl3; Schlenk technique; Sn compd. was placed in ampule; evacuated; sealed; cooled at -10°c for 30 min; BCl3 was condensed; soln. was stirred at -10°C for 1 h and at room temp. overnight; cooled to -10°C; opened to vac. for 30 min; distd. at 40°C/0.05 mbar;
参考文献
Britovsek, George J. P.; Ugolotti, Juri; White, Andrew J. P.
Organometallics, 2005 , vol. 24, # 7 p. 1685 - 1691
in hexane; toluene
under N2; soln. of BCl3 (1.00 equiv) in hexanes added to soln. of (Cu(C6F5))4(η2-toluene)2 in toluene at -78 °C; mixt. stirred at -78°C for 1 h and then allowed to gradually warm to room temp.; products not sepd.; product distribution in supernatant estimated by (19)F-NMR spectroscopy;
参考文献
Sundararaman, Anand; Jaekle, Frieder
Journal of Organometallic Chemistry, 2003 , vol. 681, # 1-2 p. 134 - 142
