反应条件
in hexane
react. 2,4,6-tri-t-butylanilidolithium with BCl3 in n-C6H14 at -78°C, then -4°C for 12 h; product filtered and crystd. at -30°C from concd. filtrate followed by sublimation; elem. anal.;
参考文献
Hitchcock, Peter B.; Jasim, Hatam A.; Lappert, Michael F.; Williams, Hugh D.
Journal of the Chemical Society, Chemical Communications, 1984 , # 10 p. 662 - 664