4-(N-苯基氨基甲基)苯硼酸频那醇酯合成路线 （共 4 条）
反应条件
caesium carbonate in N,N-dimethyl-formamide 18 h;
参考文献
INFINITY DISCOVERY, INC.
Patent: WO2008/63300 A2, 2008 ;
Location in patent: Page/Page column 215 ;
WO 2008/063300 A2
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Ma, Winson M. J.; James, Tony D.; Williams, Jonathan M. J.
Organic Letters, 2013 , vol. 15, # 18 p. 4850 - 4853
反应条件
1: toluene / 2 h / |Dean-Stark; |Reflux; |Inert atmosphere 2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether; sodium carbonate / anhydrous xylene / 24 h / 155 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
反应条件
1: toluene / 2 h / |Dean-Stark; |Reflux; |Inert atmosphere 2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether; sodium carbonate / anhydrous xylene / 24 h / 155 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
