2-甲基-4-苯基-2-丁醇合成路线 (共 84 条)
反应条件
potassium fluoride; 3-chloro-benzenecarboperoxoic acid in N,N-dimethyl acetamide T=60°C; 6 h;
参考文献
Fleming, Ian; Henning, Rolf; Plaut, Howard
Journal of the Chemical Society, Chemical Communications, 1984 , # 1 p. 29 - 31
反应条件
4-phenylbut-3-en-2-one in diethyl ether T=-50°C; 1 h; Yield given;
参考文献
Journal of the American Chemical Society, , vol. 116, # 1 p. 371 - 372
反应条件
hydrogen; palladium-copper; silica gel in ethanol T=25°C; P=760 Torr; Kinetics;
参考文献
Spee; Boersma; Meijer; Slagt; Van Koten; Geus
Journal of Organic Chemistry, 2001 , vol. 66, # 5 p. 1647 - 1656
反应条件
1: With tetrahydropyrrolo[2,1-c][1,2,4]triazole carbene; (Ph)2SiH2 in N,N-dimethyl-formamide; mineral oil T=20°C; Inert atmosphere; 2: With tetrabutyl ammonium fluoride in tetrahydrofuran; N,N-dimethyl-formamide; mineral oil T=20°C; 0.5 h; Inert atmosphere; chemoselective reaction;
参考文献
Zhao, Qiwu; Curran, Dennis P.; Malacria, Max; Fensterbank, Louis; Goddard, Jean-Philippe; Lacote, Emmanuel
Chemistry - A European Journal, 2011 , vol. 17, # 36 p. 9911 - 9914
反应条件
1: 3-phenylpropionic acid With sodium hydride in tetrahydrofuran T=20°C; 0.5 h; 2: methyl iodide With strontium in tetrahydrofuran T=20°C; 0.75 h;
参考文献
Chemistry Letters, , vol. 36, # 1 p. 28 - 29
反应条件
strontium in tetrahydrofuran T=20°C; 1 h;
参考文献
Miyoshi, Norikazu; Asaoka, Masashi; Miyazaki, Yasuaki; Tajima, Takahiro; Kikuchi, Makoto; Wada, Makoto
Chemistry Letters, 2012 , vol. 41, # 1 p. 35 - 36
参考文献
Kamitanaka, Takashi; Hikida, Tatsuyoshi; Hayashi, Satoshi; Kishida, Nobuhiro; Matsuda, Tomoko; Harada, Tadao
Tetrahedron Letters, 2007 , vol. 48, # 48 p. 8460 - 8463
参考文献
Journal of the American Chemical Society, , vol. 56, p. 185,187
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), , vol. 13, p. 222,224
Chem.Abstr., , p. 7859
反应条件
in diethyl ether T=0°C;
参考文献
Journal of the American Chemical Society, , vol. 119, # 45 p. 10947 - 10955
反应条件
4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=-78 - 0°C; 5 h;
参考文献
Yus, Miguel; Martinez, Pedro; Guijarro, David
Tetrahedron, 2001 , vol. 57, # 51 p. 10119 - 10124