2-甲基-4-苯基-2-丁醇合成路线 (共 84 条)
反应条件
1: methyl iodide With strontium in tetrahydrofuran T=20°C; 0.5 h; 2: 3-phenyl-propionaldehyde in tetrahydrofuran T=20°C; 20 h;
参考文献
Miyoshi, Norikazu; Kamiura, Koji; Oka, Hiromi; Kita, Akiko; Kuwata, Rika; Ikehara, Daitetsu; Wada, Makoto
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 2 p. 341 - 345
反应条件
cerium(III) chloride; methyllithium in tetrahydrofuran T=-78°C; 0.25 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 39, # 27 p. 4793 - 4796
反应条件
cerium(III) chloride; methyllithium in tetrahydrofuran T=-78°C; 0.25 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 39, # 27 p. 4793 - 4796
反应条件
in tetrahydrofuran T=0 - 35°C; 16 h;
参考文献
Sakai, Takahiro; Soeta, Takahiro; Inomata, Katsuhiko; Ukaji, Yutaka
Bulletin of the Chemical Society of Japan, 2012 , vol. 85, # 2 p. 231 - 235
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 44, p. 2566 - 2569,2523 - 2525
反应条件
lead(IV) acetate in Petroleum ether T=40°C; 15 h; Further byproducts given;
参考文献
Liebigs Annalen der Chemie, , # 4 p. 610 - 623
反应条件
lead(IV) acetate in Petroleum ether T=40°C; 15 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Liebigs Annalen der Chemie, , # 4 p. 610 - 623
反应条件
1: 2) H2 / 2) Ni 2: 74 percent / HBF4*Et2O / CH2Cl2 / 2 h / Ambient temperature 3: 75 percent / MCPBA, KF / N,N-dimethyl-acetamide / 6 h / 60 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 1 p. 29 - 31
反应条件
lead(IV) acetate in acetic acid T=50°C; 19 h; Further byproducts given;
参考文献
Liebigs Annalen der Chemie, , # 4 p. 610 - 623
参考文献
Journal of the American Chemical Society, , vol. 88, p. 5809 - 5816