2-甲基-4-苯基-2-丁醇合成路线 (共 84 条)
参考文献
Kamitanaka, Takashi; Hikida, Tatsuyoshi; Hayashi, Satoshi; Kishida, Nobuhiro; Matsuda, Tomoko; Harada, Tadao
Tetrahedron Letters, 2007 , vol. 48, # 48 p. 8460 - 8463
反应条件
1: boron trifluoride diethyl etherate / 5 h / 40 - 46 °C / |Inert atmosphere 2: hydrogen; 5 palladium on charcoal; phosphoric acid / 36 h / 80 - 105 °C / 7500.75 - 11251.1 Torr / |Inert atmosphere; |Autoclave; |Large scale View Scheme
参考文献
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 47, p. 2049
Chem. Zentralbl., , vol. 87, # II p. 384
参考文献
Journal of Organic Chemistry, , vol. 28, p. 1960 - 1968
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 105, p. 72
Chemische Berichte, , vol. 58, p. 279 Anm. 15
反应条件
lithium aluminium tetrahydride; (tBuOOCO)2; oxygen 1.) benzene, 45 deg C, 4 h, 2.) THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
South African Journal of Chemistry, , vol. 50, # 1 p. 1 - 8
参考文献
Tetrahedron, , vol. 42, # 5 p. 1487 - 1496
参考文献
Helvetica Chimica Acta, , vol. 64, # 3 p. 835 - 843
反应条件
lithium aluminium tetrahydride; oxygen T=90°C; P=101.3 Torr; 5 h; autoxidation; Product distribution;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 326, # 1 p. 73 - 80
反应条件
2,6-dimethylpyridine; water in 1,4-dioxane T=80°C; 14 h; Product distributionMechanism;
参考文献
Chemische Berichte, , vol. 113, # 6 p. 2140 - 2153
反应条件
Multistep reaction; the efficiency of LMPA as in situ carbonyl protecting group of aldehydes were investigated beside carboxylic esters and nitriles against organometallic reagents or LAH; Product distribution;
参考文献
Comins, Daniel L.; Brown, Jack D.
Tetrahedron Letters, 1981 , vol. 22, # 42 p. 4213 - 4216