2-甲基-4-苯基-2-丁醇合成路线 （共 84 条）
反应条件
epoxysulfonyl fluoride in dichloromethane
T=-78°C; 0.5 h;
参考文献
Bright; Coxon; Steel
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1338 - 1344
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Barrow, Colin J.; Bright, Steven T.; Coxon, James M.; Steel, Peter J.
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2542 - 2549
反应条件
phosphoric acid, fully deuterated
T=230 - 240°C; 3 h; Yield given. Title compound not separated from byproducts;
参考文献
Sakhabutdinov, A. G.; Usmanova, A. G.; Frolov, P. A.; Kushnarev, D. F.; Schmidt, F. K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 8 p. 1452 - 1455
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1610 - 1614
参考文献
Bogert; Davidson
Journal of the American Chemical Society, 1934 , vol. 56, p. 185,187
反应条件
hydrogen in tetrahydrofuran
T=200°C; P=150015 Torr; 6 h; Autoclave; Catalytic behavior; Time;
参考文献
BASF SE; Schuch, Rudolf; Rüdenauer, Stefan; Ebel, Klaus; Pelzer, Ralf; Keller, Andreas
Patent: US2013/72726 A1, 2013 ;
Location in patent: Paragraph 0108-0109 ;
