1: 100 percent / [Cl(C6F13C2H4)2SnOSn(C2H4C6F13)2Cl]2 / various solvent(s) / 16 h / 150 °C 2: 96 percent / [Cl(C6F13C2H4)2SnOSn(C2H4C6F13)2Cl]2 / various solvent(s); toluene / 16 h / 150 °C 3: 100 percent / [Cl(C6F13C2H4)2SnOSn(C2H4C6F13)2Cl]2 / various solvent(s) / 16 h / 150 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 344, # 1 p. 84 - 90
triethyl borane in hexane; benzene addn. of hexane soln. of Et3B to a soln. of methyl cinnamate and Bu3SnH in benzene at 25°C under Ar, stirring for 15 h at 25°C; concn. in vac., chromy. on silica gel (hexane/ethyl acetate);
参考文献
Bulletin of the Chemical Society of Japan, , vol. 64, # 8 p. 2585 - 2587