反应条件
CH3MgBr in diethyl ether Methylation of reaction mixture with MeMgBr in Et2O at 0°C with stirring for 0.5 h, then stirring of the mixture at room temp. for 1 h under Ar.; addn. of H2O and NH4Cl, sepn. of phases, extn. of aq. phase (Et2O), removal of solvent, pptn. of tetraphenylnaphthalene (pentane), investigation of crude products by GC-MS anal.;
参考文献
Koecher, Juergen; Lehnig, Manfred; Neumann, Wilhelm P.
Organometallics, 1988 , vol. 7, p. 1201 - 1207
