1: ethyl acetoacetate With sodium ethanolate in ethanol
T=60°C; 0.5 h;
2: 2-(phenyl)ethyl bromide in ethanol
16 h; Heating / reflux;
3: With hydrogenchloride in water
pH=3;
参考文献
INSTITUT NATIONAL DE LA SANTE ET DE LA RECHERCHE MEDICALE (INSERM)
Patent: EP1683790 A1, 2006 ;
Location in patent: Page/Page column 7; 11 ;
EP 1683790 A1
Heilbron et al.
Journal of the Chemical Society, 1931 , p. 1336,1340
Full Text Show Details
Ramart-Lucas; Labaune
Annales de Chimie (Cachan, France), 1931 , vol. <10> 16, p. 276,298