NiCRA-bpy (2/2/1/2) in ethylene glycol dimethyl ether T=65°C; 18 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 55, # 25 p. 6194 - 6198
1: With sodium azide in 1-methyl-pyrrolidin-2-one; water T=70°C; 3 h; 2: With sodium tetrahydroborate in 1-methyl-pyrrolidin-2-one; water T=50 - 70°C; 3 h;
参考文献
Torisawa, Yasuhiro; Nishi, Takao; Minamikawa, Jun-ichi
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 8 p. 2583 - 2587
H-mordenite zeolite (Si/Al ratio of 41.6, Na level of 130 ppm) mixed with alumina, pore forming reagent and extruded to form 1/12-inch cylindrical pellets (80percent sieve/20percent binder), calcined, mixed with ammonium heptamolybdate/water; impregnated catalyst (2percent Mo) calcined at 500° C. (1-3 h); macropore volume (>50 nm) = 0.288 cc/g T=382.212 - 398.879°C; P=11103.3 Torr; Product distribution / selectivity;
