lithium aluminium tetrahydride; meta-chloroperoxybenzoic acid 2.) ether, 30 min, reflux; study of the regioselectivity of autoxidation by reduction of the corresponding oxidation-mixture; MechanismProduct distribution;
H-mordenite zeolite (Si/Al ratio of 41.6, Na level of 130 ppm) mixed with alumina, pore forming reagent and extruded to form 1/12-inch cylindrical pellets (80percent sieve/20percent binder), calcined, mixed with ammonium heptamolybdate/water; impregnated catalyst (2percent Mo) calcined at 500° C. (1-3 h); macropore volume (>50 nm) = 0.288 cc/g T=343.323 - 412.768°C; P=11103.3 Torr; Product distribution / selectivity;
参考文献
Schwartz, Hilary E.; Miller, Jeffrey T.; Henley, Brian J.; Huff, George A.
Patent: US2007/49780 A1, 2007 ;
Location in patent: Page/Page column 20-21 ;
H-mordenite zeolite (Si/Al ratio of 41.6, Na level of 130 ppm) mixed with alumina, pore forming reagent and extruded to form 1/12-inch cylindrical pellets (80percent sieve/20percent binder), calcined, mixed with ammonium heptamolybdate/water; impregnated catalyst (2percent Mo) calcined at 500° C. (1-3 h); macropore volume (>50 nm) = 0.280 cc/g T=359.99°C; P=11103.3 Torr; Product distribution / selectivity;
参考文献
Schwartz, Hilary E.; Miller, Jeffrey T.; Henley, Brian J.; Huff, George A.
Patent: US2007/49780 A1, 2007 ;
Location in patent: Page/Page column 22-23 ;
