反应条件
1.1: triethylamine / dichloromethane / 15 h / 20 °C / |Inert atmosphere 2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / |Inert atmosphere 2.2: 15 h / 0 - 20 °C / |Inert atmosphere 3.1: sec.-butyllithium / tetrahydrofuran / -78 °C / |Inert atmosphere View Scheme
参考文献
Fournier, Anne M.; Nichols, Christopher J.; Vincent, Mark A.; Hillier, Ian H.; Clayden, Jonathan
Chemistry - A European Journal, 2012 , vol. 18, # 51 p. 16478 - 16490