Whitmore; Fleming
Journal of the American Chemical Society, 1933 , vol. 55, p. 4162
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Underwood; Gale
Journal of the American Chemical Society, 1934 , vol. 56, p. 2117,2119
1: phenylacetylene With Di-n-butylmagnesium in tetrahydrofuran; n-heptane
1 h; Inert atmosphereGlovebox;
2: phenyl isocyanate in tetrahydrofuran; n-heptane
Inert atmosphereGlovebox;
参考文献
Hill, Michael S.; Liptrot, David J.; Mahon, Mary F.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 20 p. 5364 - 5367
Angew. Chem., 2013 , vol. 125, # 20 p. 5472 - 5475,4
T=160 - 180°C; der Aethylester entsteht; man behandelt den entstandenen Aethylester mit 10prozentiger Natronlauge in der Kaelte;
参考文献
Lambling
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1898 , vol. 127, p. 66
Bulletin de la Societe Chimique de France, 1898 , vol. <3>19, p. 772