1.) educt preheated in acetone at 60 deg C for 2 h before adding reagent, 2.) room temperature, 1 d; other solvents: CDCl3, CD3CN, acetone-d6; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
L'abbe, Garrit; Buelens, Karin
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 7 p. 1993 - 1995
in chloroform-d1
72 h; Ambient temperatureeduct preheated in solution at 60 deg C for 2 h before adding reagent; other solvent: deuterated acetonitrile; analyzed by 1H nmr spectroscopy; Product distribution;
参考文献
L'abbe, Garrit; Buelens, Karin
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 7 p. 1993 - 1995
