in 1,2-dichloro-ethane addn.of PhNCS to a soln. of the Sn-compound under N2; stirred at 40°C for 2 h; solvent was removed in vac.; column chromy. (silica gel; eluent: C6H6); vac. distn. (120°C/0.1 Torr);
triethylamine in 1,2-dichloro-ethane addn.of PhNCS to a soln. of the Sn-compound and Et3N under N2; stirred at 40°C for 5.0 h; solvent was removed in vac.; column chromy. (silica gel; eluent: C6H6); vac. distn.;
in 1,2-dichloro-ethane addn.of PhNCS to a soln. of the Sn-compounds under N2; stirred at 40°C for 1.0 h; solvent was removed in vac.; column chromy. (silica gel; eluent: C6H6); vac. distn.;
Khan, Khalid Mohammed; Naz, Farzana; Taha, Muhammad; Khan, Ajmal; Perveen, Shahnaz; Choudhary; Voelter, Wolfgang
European Journal of Medicinal Chemistry, 2014 , vol. 74, p. 314 - 323