1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C 1.2: 1 h / -78 - 20 °C 2.1: lithium hexamethyldisilazane / hexane; tetrahydrofuran / 0.5 h / -78 °C 2.2: 12 h / -78 - 20 °C 3.1: lithium hydroxide hydrate; water / tetrahydrofuran / 12 h / 20 °C View Scheme
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Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1819 - 1828