1: 774 g / sodium ethoxide / ethanol / 4 h / Heating
2: 446 g / potassium t-butoxide / 2-methyl-propan-2-ol / 1 h / Heating
View Scheme
参考文献
Thuring, Jan Willem J. F.; Van Gaal, Angelique A. M. A.; Hornes, Sander J.; De Kok, Margreet M.; Nefkens, Gerard H. L.; Zwanenburg, Binne
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 767 - 774
1: SOCl2 / 1,2-dichloro-ethane / 3 h / 80 °C
2: 1,2-dichloro-ethane / 0.25 h / Ambient temperature
3: AlCl3 / 1,2-dichloro-ethane / 1 h / 80 °C
View Scheme
参考文献
Venkov, A. P.; Mollov, N. M.
Synthesis, 1982 , # 3 p. 216 - 217