CO in tetrahydrofuran dissolving of the cluster in THF, degassing (three freeze-pump-thaw cycles), placing under 1 atm of CO (room temp., 1 d); evapn. of solvent, chromy. (silica gel, hexane);
1: phenyl trimethoxy silane With tetrabutyl ammonium fluoride; copper diacetate; RF-PPh3 in dichloromethane; water T=20°C; 0.0833333 h; Molecular sieve; 2: acetamide With oxygen in dichloromethane; water T=20°C; 24 h;
参考文献
Lin, Baoda; Liu, Miaochang; Ye, Zhishi; Ding, Jinchang; Wu, Huayue; Cheng, Jiang
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 5 p. 869 - 873
