4-(2-氨基丙基)苯酚合成路线 （共 19 条）
反应条件
1: 80 percent / H2 / 5 percent Pt/C / ethanol / 12 h / 20 °C / 3750.3 Torr 2: 60 percent / H2; HCOOH / 10 percent Pd/C / ethanol / 6 h / 20 °C / 2250.18 Torr View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 13, # 16 p. 2687 - 2692
反应条件
formic acid; hydrogen; 10 palladium on active carbon in ethanol T=20°C; P=2250.18 Torr; 6 h;
参考文献
Schirrmacher, Esther; Schirrmacher, Ralf; Thews, Oliver; Dillenburg, Wolfgang; Helisch, Andreas; Wessler, Ignatz; Buhl, Roland; Hoehnemann, Sabine; Buchholz, Hans-Georg; Bartenstein, Peter; Machulla, Hans-Juergen; Roesch, Frank
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 16 p. 2687 - 2692
反应条件
hydrogen; palladium on activated charcoal in perchloric acid; water; acetic acid P=3900.3 Torr; 14.5 h; Ambient temperature;
参考文献
Rucker; Neugebauer; Heiden
Arzneimittel-Forschung/Drug Research, 1988 , vol. 38, # 4 p. 497 - 501
反应条件
hydrogen bromide in water 3 h; Reflux;
参考文献
Munoz, Lourdes; Rodriguez, Anna M.; Rosell, Gloria; Bosch, M. Pilar; Guerrero, Angel
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8171 - 8177
反应条件
1: pentylamine / 20 °C 2: ethanol; acetic acid; aqueous sulfuric acid / bei der elektrochemischen Reduktion 3: aqueous hydrochloric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 54, p. 271,273
反应条件
1: sodium hydroxide; aqueous ammonia 2: bromine; aqueous KOH-solution / anschliessend Erwaermen des mit Natriumhydroxid versetzten Reaktionsgemisches 3: aqueous hydrochloric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 60, p. 465
反应条件
1: bromine; aqueous KOH-solution / anschliessend Erwaermen des mit Natriumhydroxid versetzten Reaktionsgemisches 2: aqueous hydrochloric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 60, p. 465
反应条件
1: ethanol; acetic acid; aqueous sulfuric acid / bei der elektrochemischen Reduktion 2: aqueous hydrochloric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 54, p. 271,273
反应条件
1: lithium aluminium tetrahydride / diethyl ether / 3 h / Inert atmosphere; Reflux 2: hydrogen bromide / water / 3 h / Reflux View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 23 p. 8171 - 8177
反应条件
hydrogenchloride; sodium nitrite anschliessend Erwaermen auf 70grad;
参考文献
Journal of Organic Chemistry, , vol. 12, p. 501,504
