反应条件
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.08 h / 0 °C / |Inert atmosphere 1.2: 14 h / 20 °C / |Inert atmosphere 2.1: tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; sodium t-butanolate / toluene / 12 h / 80 °C / |Inert atmosphere; |Schlenk technique 3.1: sodium acetate; hydroxylamine hydrochloride / methanol / 1 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Wang, Xi; Xu, Yan; Mo, Fanyang; Ji, Guojing; Qiu, Di; Feng, Jiajie; Ye, Yuxuan; Zhang, Songnan; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2013 , vol. 135, # 28 p. 10330 - 10333