反应条件
Multi-step reaction with 5 steps 1: 18.1 g / 5percent NaOH aq. / methanol; CH2Cl2 / 1 h / Ambient temperature2: 21.7 g / pyridine / 1 h / Ambient temperature3: 80 percent / LiBr / dimethylformamide / 1 h / 140 °C4: 14.8 g / OsO4, N-methylmorpholine N-oxide, H2O / 2-methyl-propan-2-ol; tetrahydrofuran / 2 h / Ambient temperature5: 88 percent / p-toluenesulfonic acid / 2 h / Ambient temperature
参考文献
Kametani; Katoh; Fujio; Nogiwa; Tsubuki; Honda Journal of Organic Chemistry, 1988 , vol. 53, # 9 p. 1982 - 1991
