反应条件
1: 87 percent / AG 50W-X4 / CH2Cl2; methanol / 1 h / Ambient temperature 2: 93 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature 3: 98 percent / CH2Cl2 / 18 h / Ambient temperature 4: 1.) n-BuLi / 1.) THF, n-hexane, -78 deg C, 5 min, 2.) THF, n-hexane, -78 deg C, 2 h View Scheme
参考文献
Baggiolini, Enrico G.; Iacobelli, Jerome A.; Hennessy, Bernard M.; Batcho, Andrew D.; Sereno, John F.; Uskokovic, Milan R.
Journal of Organic Chemistry, 1986 , vol. 51, # 16 p. 3098 - 3108
