反应条件
HCl in dichloromethane byproducts: HSi(C6H5)3, P(C6H5)2CH3; passing a stream of dry HCl through Ag complex soln. at -40°C up to decoloration; heating to room temp.; evapn. in high vac.; all operations under N2; vigorously stirring with petroleum ether; filtration of powder; washing with petroleum ether; drying in high vac.; spectroscopic detn. of PPh2Tol and Ph3SiH in filtrate;
参考文献
Wagner, Herbert; Schubert, Ulrich
Chemische Berichte, 1990 , vol. 123, p. 2101 - 2108
