1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C
1.2: 5 h / 0 °C
2.1: sodium methylate / water / 6 h / 70 °C
3.1: sodium hydroxide / tetrahydrofuran; water / 20 °C
View Scheme
参考文献
Maslyk, MacIej; Zapico, Jose M.; Swider, Robert; Martin-Santamaria, Sonsoles; Ramos, Ana; De Pascual-Teresa, Beatriz
Arkivoc, 2011 , vol. 2011, # 3 p. 54 - 71
Balu, Narayanan; Gamcsik, Michael P.; Colvin, Michael E.; Colvin, O. Michael; Dolan, M. Eileen; Ludeman, Susan M.
Chemical Research in Toxicology, 2002 , vol. 15, # 3 p. 380 - 387
1: 90 percent / dimethylsulfoxide / 12 h / Ambient temperature
2: 87 percent / NaH / dimethylsulfoxide / 1.) r.t., 1 h, 2.) r.t., 12 h
View Scheme
参考文献
Lembicz, Nicola K.; Grant, Sharon; Clegg, William; Griffin, Roger J.; Heath, Sarah L.; Golding, Bernard T.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 3 p. 185 - 186
