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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-氨基-6-氯嘌呤
合成路线
（共 140 条）
10310-21-1
2-氨基-6-氯嘌呤
→
反应条件
104227-87-4
泛昔洛韦
反应条件
1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 12 h / 70 °C / Inert atmosphere 2: potassium carbonate / dimethyl sulfoxide / 4 h / 40 - 50 °C 3: palladium 10 on activated carbon; hydrogen; triethylamine / methanol / 7 h / 55 °C 4: methanol; sodium tetrahydroborate / dichloromethane / 2.5 h / 20 °C 5: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 12 h / 20 °C View Scheme
参考文献
Heterocycles, , vol. 75, # 11 p. 2803 - 2808
10310-21-1
2-氨基-6-氯嘌呤
→
反应条件
103884-98-6
9-(2-脱氧-2-氟阿拉伯呋喃基)鸟嘌呤
反应条件
1: ammonium sulfate / 1.5 h / Heating 2: 1.) Hg(CN)2 / 1.) C6H6, reflux, 30 min, 2.) reflux, 3.4 h 3: 1 M Bu4NF / CH2Cl2; tetrahydrofuran / 0.25 h 4: 20 percent / 0.5 N aq. NaOH / dioxane / 1 h / 100 °C View Scheme
参考文献
Borthwick; Kirk; Biggadike; Exall; Butt; Roberts; Knight; Coates; Ryan
Journal of Medicinal Chemistry, 1991 , vol. 34, # 3 p. 907 - 914
10310-21-1
2-氨基-6-氯嘌呤
→
反应条件
118353-05-2
卡巴韦
反应条件
1: 2) sodium hydride / 1) CH3CN, 2) DMF 2: sodium periodate 3: 26 percent / calcium carbonate, norbornene / various solvent(s) / Heating 4: 76 percent / TBAF 5: 81 percent / 0.5N aq. NaOH / 3 h / Heating View Scheme
参考文献
Gundersen, Lise-Lotte; Benneche, Tore; Rise, Frode; Gogoll, Adolf; Undheim, Kjell
Acta Chemica Scandinavica, 1992 , vol. 46, # 8 p. 761 - 771
108321-99-9
二钠5-O-膦酸基-D-核酮糖
+
10310-21-1
2-氨基-6-氯嘌呤
→
反应条件
2004-07-1
6-氯鸟嘌呤核苷
反应条件
2-hydroxyethanethiol; manganese (II) chloride; purine nucleoside phosphorylase in various solvent(s) T=45°C; pH=7; 32 h;
参考文献
Taverna-Porro, Marisa; Bouvier, Leon A.; Pereira, Claudio A.; Montserrat, Javier M.; Iribarren, Adolfo M.
Tetrahedron Letters, 2008 , vol. 49, # 16 p. 2642 - 2645
81100-62-1
+
10310-21-1
2-氨基-6-氯嘌呤
→
反应条件
2004-07-1
6-氯鸟嘌呤核苷
+
578-76-7
7-甲基鸟嘌呤
反应条件
recombinant purine nucleoside phosphorylase from Aeromonas hydrophila T=20°C; pH=7.5; aq. phosphate bufferEnzymatic reaction; regioselective reaction;
参考文献
Ubiali, Daniela; Serra, Carla D.; Serra, Immacolata; Morelli, Carlo F.; Terreni, Marco; Albertini, Alessandra M.; Manitto, Paolo; Speranzab, Giovanna
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 1 p. 96 - 104
10310-21-1
2-氨基-6-氯嘌呤
→
反应条件
2004-07-1
6-氯鸟嘌呤核苷
反应条件
1: N,O-bis(trimethylsilyl)acetamide; trimethylsilyl triflate / acetonitrile / 0.08 h / 130 °C / microwave irradiation 2: NH3 / 16 h / 50 °C View Scheme
参考文献
Xie, Lujia; Yang, Xiantao; Pan, Delin; Cao, Yingli; Cao, Mou; Lin, Guichun; Guan, Zhu; Guo, Ying; Zhang, Lihe; Yang, Zhenjun
Chinese Journal of Chemistry, 2013 , vol. 31, # 9 p. 1207 - 1218
10310-21-1
2-氨基-6-氯嘌呤
+
58-96-8
尿嘧啶核苷
→
反应条件
2004-07-1
6-氯鸟嘌呤核苷
反应条件
aeromonas hydrophila CECT 4226 T=60°C; pH=7; 2 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Nbile, Matas; Terreni, Marco; Lewkowicz, Elizabeth; Iribarren, Adolfo M.
Biocatalysis and Biotransformation, 2010 , vol. 28, # 5-6 p. 395 - 402
10310-21-1
2-氨基-6-氯嘌呤
→
反应条件
2096-10-8
2,6-二氨基嘌呤核苷
反应条件
1: N,O-bis(trimethylsilyl)acetamide; trimethylsilyl triflate / acetonitrile / 0.08 h / 130 °C / microwave irradiation 2: NH3 / 16 h / 50 °C View Scheme
参考文献
Bookser, Brett C.; Raffaele, Nicholas B.
Journal of Organic Chemistry, 2007 , vol. 72, # 1 p. 173 - 179
10310-21-1
2-氨基-6-氯嘌呤
→
反应条件
32976-84-4
反应条件
1: 1) sodium hydride (60percent in oil) / 1) acetonitrile, RT, 30 min; 2) acetonitrile, RT, 15 h 2: 62 percent / boron trichloride / CH2Cl2 / 1) -78 deg C, 4 h; 2) from -20 deg C to -30 deg C, 2 h 3: 74 percent / sodium hydrosulfide hydrate / ethanol / 6 h / Heating View Scheme
参考文献
Hanna; Ramasamy; Robins; Revankar
Journal of Heterocyclic Chemistry, 1988 , vol. 25, # 6 p. 1899 - 1903
→
反应条件
35095-93-3
2-氨基-6-氯-9-(3,5-二-邻(对甲苯)-beta-d-2-脱氧呋喃核糖)嘌呤
反应条件
in dichloromethane; acetonitrile
参考文献
ISIS Pharmaceuticals, Inc.
Patent: US5681941 A1, 1997 ;
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