反应条件
Stage #1: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1619616', constants.ctx, '0')">18-crown-6 ether</a>; <a href="#" onclick="return RXDsubstances(event, this, '4122952', constants.ctx, '0')">sodium hydride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br />T=20 - 60°C; 1 h; Cooling with ice; <br />Stage #2: <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1098214', constants.ctx, '0')">hydrogenchloride</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1718733', constants.ctx, '0')">ethanol</a>; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a>; <a href="#" onclick="return RXDsubstances(event, this, '635760', constants.ctx, '0')">toluene</a> <br />T=65°C; pH=4; 2 h; <br /> <br />
参考文献
Khose, Goraksha; Shinde, Shailesh; Panmand, Anil; Kulkarni, Ravibhushan; Munot, Yogesh; Bandyopadhyay, Anish; Barawkar, Dinesh; Patil, Santoshkumar N. Tetrahedron Letters, 2014 , vol. 55, # 16 p. 2671 - 2674
