4-(4-乙酰基-2-甲氧基-5-硝基苯氧基)丁酸乙酯合成路线 (共 5 条)
反应条件
nitric acid in acetic anhydride T=0°C; 3 h;
参考文献
Qvortrup, Katrine; Nielsen, Thomas E.
Chemical Communications, 2011 , vol. 47, # 11 p. 3278 - 3280
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 19 h / 20 - 50 °C 2: nitric acid / acetic anhydride / 3 h / 0 °C View Scheme
参考文献
Griffin, Donald R.; Kasko, Andrea M.
Journal of the American Chemical Society, 2012 , vol. 134, # 31 p. 13103 - 13107
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 25 °C / Inert atmosphere 2: nitric acid / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
The Regents of the University of Colorado, A Body Corporate
Patent: US8343710 B1, 2013 ;
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 50 °C 2: acetic anhydride; nitric acid / 5 h / |Cooling with ice View Scheme
参考文献
Yan, Bin; Boyer, John-Christopher; Habault, Damien; Branda, Neil R.; Zhao, Yue
Journal of the American Chemical Society, 2012 , vol. 134, # 40 p. 16558 - 16561
反应条件
1: sodium tetrahydroborate 2: water; sodium hydroxide View Scheme
参考文献
Soft Matter, , vol. 7, # 10 p. 4881 - 4887