2-(1-苯基乙酮-2-基)异吲哚啉-1,3-二酮合成路线 （共 30 条）
参考文献
Gabriel
Chemische Berichte, 1908 , vol. 41, p. 1143
Chemische Berichte, 1913 , vol. 46, p. 3860
Full Text Show Details
Goedeckemeyer
Chemische Berichte, 1888 , vol. 21, p. 2686
反应条件
1: 88 percent / toluene-p-sulphonic acid / toluene / 1.5 h / Heating 2: 92 percent / thionyl chloride / Ambient temperature 3: 79 percent / hydrazine hydrate / ethanol / Heating View Scheme
参考文献
Masuda, Katsutada; Adachi, Jun; Nate, Hiroyuki; Takahata, Hidenobu; Nomura, Keiichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1591 - 1595
反应条件
1: alcoholic potash 2: hydrochloric acid View Scheme
参考文献
Gabriel
Chemische Berichte, 1908 , vol. 41, p. 1143
Chemische Berichte, 1913 , vol. 46, p. 3860
Full Text Show Details
Goedeckemeyer
Chemische Berichte, 1888 , vol. 21, p. 2686
反应条件
1: sodium cyanoborohydride; acetic acid / 24 h / 20 °C 2: hydrazine hydrate / water / 3 h / 60 °C View Scheme
参考文献
Gupta, Pankaj; Rouf, Abdul; Shah, Bhahwal A.; Mukherjee, Debaraj; Taneja, Subhash C.
Synthetic Communications, 2013 , vol. 43, # 4 p. 505 - 519
反应条件
in isobutyramide; water
T=18 - 40°C; 5 h;
参考文献
FUJIFILM CORPORATION
Patent: US2012/238752 A1, 2012 ;
Location in patent: Page/Page column 37 ;
反应条件
in N,N-dimethyl-formamide
0.5 h; Heating;
参考文献
Gupta, Pankaj; Rouf, Abdul; Shah, Bhahwal A.; Mukherjee, Debaraj; Taneja, Subhash C.
Synthetic Communications, 2013 , vol. 43, # 4 p. 505 - 519
反应条件
potassium carbonate in etnanol
T=20°C; 96 h;
参考文献
Gerpe, Alejandra; Bollini, Mariela; Gonzalez, Mercedes; Cerecetto, Hugo
Synthetic Communications, 2009 , vol. 39, # 1 p. 29 - 47
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
T=20°C; 12 h;
参考文献
Wei, Ying; Lin, Shaoxia; Liang, Fushun
Organic Letters, 2012 , vol. 14, # 16 p. 4202 - 4205
反应条件
tetrakis(triphenylphosphine) palladium(0); copper (I) cyanide in toluene
T=75°C; Stille Cross Coupling; 20 h; Inert atmosphere;
参考文献
Malova Krizkova, Petra; Hammerschmidt, Friedrich
European Journal of Organic Chemistry, 2013 , # 23 p. 5143 - 5148
反应条件
in N,N-dimethyl-formamide
T=20°C; 4 h;
参考文献
SANOFI
Patent: US2012/115898 A1, 2012 ;
Location in patent: Page/Page column 17 ;
