2,6-二苯基四氢噻喃-4-酮S,S-二氧化物合成路线 (共 5 条)
反应条件
1: 3 percent / I2, DMSO, H2SO4 / 2 h / 100 °C 2: K2HPO4, NaHS*2H2O / propan-2-ol; H2O / Ambient temperature View Scheme
参考文献
Rule; Detty; Kaeding; Sinicropi
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1665 - 1673
反应条件
1: 3 percent / I2, DMSO, H2SO4 / 2 h / 100 °C 2: K2HPO4, NaHS*2H2O / propan-2-ol; H2O / Ambient temperature View Scheme
参考文献
Rule; Detty; Kaeding; Sinicropi
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1665 - 1673
反应条件
sulfuric acid; iodine; dimethyl sulfoxide T=100°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 60, # 6 p. 1665 - 1673
反应条件
sulfuric acid; iodine in dimethyl sulfoxide
24 h; Heating; Yield given;
参考文献
Chen, Chin H.; Reynolds, George A.; Luss, H. R.; Perlstein, Jerome H.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3282 - 3289
反应条件
sulfuric acid; iodine; dimethyl sulfoxide
T=100°C; 2 h;
参考文献
Rule; Detty; Kaeding; Sinicropi
Journal of Organic Chemistry, 1995 , vol. 60, # 6 p. 1665 - 1673