反应条件
in neat (no solvent)
Teflon-valve-equipped standard vacuum line or a nitrogen-filled glovebox;3 aliquots of BBr3 added to BCl2B5H8, stirred, while reactor was held at -78 ° C, volatile material removed at -78 ° C, reactor warmed to -10 ° C; fractionation,identification by boron NMR and mass spectroscopy; small amts. of B2H6, BCl2H, BBr2H, and mixed boron trihalides;
参考文献
Saulys, D. A.; Morrison, J. A.
Inorganic Chemistry, 1990 , vol. 29, p. 4174 - 4179
