反应条件
1: tert-butyl (S)-1-(N-benzyl-N-methylcarbamoyl)-2,2-dimethylpropylcarbamate With hydrogenchloride in 1,4-dioxane
T=20°C; 2 h;
2: 3,5-bis(trifluoromethyl)phenyl isothiocyanate With triethylamine in dichloromethane
T=20°C; 4 h; Further stages.;
参考文献
Reisman, Sarah E.; Doyle, Abigail G.; Jacobsen, Eric N.
Journal of the American Chemical Society, 2008 , vol. 130, # 23 p. 7198 - 7199