反应条件
1: 56 percent / lithium di-isopropylamide, HMPA / tetrahydrofuran 2: 88 percent / KOH / methanol / 16 h / Ambient temperature 3: 20 percent / Et3N, diphenylphosphoryl azide / toluene / 7 h / Heating 4: Heating 5: 1.) O3; 2.) NaBH4 / 1.) CH2Cl2, -15 deg C, 8 min; 2.) EtOH, 0 deg C, 1.5 h View Scheme
参考文献
Miles, Nicholas J.; Sammes, Peter G.; Kennewell, Peter D.; Westwood, Robert
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 2299 - 2306
