N-(芴甲氧羰基)甘氨酰氯合成路线 （共 8 条）
反应条件
thionyl chloride; N,N-dimethyl-formamide in dichloromethane 1 h; Ambient temperature;
参考文献
Carpino, Louis A.; Cohen, Beri J.; Stephens, Kenton E.; Sadat-Aalaee, S. Yahya; Tien, Jien-Heh; Langridge, Denton C.
Journal of Organic Chemistry, 1986 , vol. 51, # 19 p. 3732 - 3734
反应条件
N,N-dimethyl-formamide in dichloromethane Substitution; 1.5 h; Heating;
参考文献
Organic letters, , vol. 2, # 10 p. 1399 - 1401
反应条件
1: zinc / tetrahydrofuran / 20 °C 2: water; calcium chloride; sodium hydroxide / isopropyl alcohol View Scheme
参考文献
Ramesh; Raju; Srinivas; Sureshbabu; Vishwanatha; Hemantha
Rapid Communications in Mass Spectrometry, 2011 , vol. 25, # 14 p. 1949 - 1958
反应条件
pyridine in tetrahydrofuran T=4°C;
参考文献
Tetrahedron Letters, , vol. 32, # 43 p. 6199 - 6202
反应条件
sodium azide in acetone T=0°C; 0.25 h;
参考文献
Vasanthakumar, Ganga-Ramu; Ananda, Kuppanna; Suresh Babu, Vommina V
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 8 p. 1733 - 1735
反应条件
tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Ambient temperature;
参考文献
Salvi, Jean-Paul; Walchshofer, Nadia; Paris, Joelle
Tetrahedron Letters, 1994 , vol. 35, # 8 p. 1181 - 1184
反应条件
1: zinc / tetrahydrofuran / 20 °C
2: water; calcium chloride; sodium hydroxide / isopropyl alcohol
View Scheme
参考文献
Ramesh; Raju; Srinivas; Sureshbabu; Vishwanatha; Hemantha
Rapid Communications in Mass Spectrometry, 2011 , vol. 25, # 14 p. 1949 - 1958
反应条件
sodium hydrogencarbonate in dichloromethane
10 h; Yield given. Further byproducts given;
参考文献
Carpino, Louis A.; Sadat-Aalaee, Dean; Beyermann, Michael
Journal of Organic Chemistry, 1990 , vol. 55, # 5 p. 1673 - 1675
