N-[(1S)-1-(氯甲酰基)乙基]氨基甲酸芴甲基酯合成路线 (共 6 条)
反应条件
thionyl chloride in dichloromethane T=60°C; 0.5 h; Inert atmosphere;
参考文献
Laungani, Andy C.; Slattery, John M.; Krossing, Ingo; Breit, Bernhard
Chemistry - A European Journal, 2008 , vol. 14, # 15 p. 4488 - 4502
反应条件
N,N-dimethyl-formamide in dichloromethane Substitution; 1.5 h; Heating;
参考文献
Organic letters, , vol. 2, # 10 p. 1399 - 1401
反应条件
pyridine in tetrahydrofuran T=4°C;
参考文献
Jacobsen, Mogens Havsteen; Buchardt, Ole; Engdahl, Tom; Holm, Arne
Tetrahedron Letters, 1991 , vol. 32, # 43 p. 6199 - 6202
反应条件
1: 93 percent / CH2Cl2 / 1 h / Ambient temperature 2: 90 percent / silver benzoate / dioxane; H2O / 70 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 13 p. 1969 - 1971
反应条件
1: zinc / tetrahydrofuran / 20 °C
2: water; calcium chloride; sodium hydroxide / isopropyl alcohol
View Scheme
参考文献
Ramesh; Raju; Srinivas; Sureshbabu; Vishwanatha; Hemantha
Rapid Communications in Mass Spectrometry, 2011 , vol. 25, # 14 p. 1949 - 1958
反应条件
aluminium trichloride
T=20°C;
参考文献
Di Gioia, Maria Luisa; Leggio, Antonella; Le Pera, Adolfo; Liguori, Angelo; Siciliano, Carlo
European Journal of Organic Chemistry, 2004 , # 3 p. 463 - 467