N-[(1S)-2-氯-2-氧代-1-(苯甲基)乙基]-氨基甲酸-9H-芴-9-甲酯合成路线 (共 7 条)
反应条件
thionyl chloride; N,N-dimethyl-formamide in dichloromethane 1 h; Ambient temperature;
参考文献
Carpino, Louis A.; Cohen, Beri J.; Stephens, Kenton E.; Sadat-Aalaee, S. Yahya; Tien, Jien-Heh; Langridge, Denton C.
Journal of Organic Chemistry, 1986 , vol. 51, # 19 p. 3732 - 3734
反应条件
1: sodium carbonate / acetone 2: thionyl chloride / dichloromethane View Scheme
参考文献
RSC Advances, , vol. 3, # 32 p. 13412 - 13416
反应条件
1: sodium carbonate / acetone 2: thionyl chloride / dichloromethane View Scheme
参考文献
RSC Advances, , vol. 3, # 32 p. 13412 - 13416
反应条件
pyridine in tetrahydrofuran T=4°C;
参考文献
Jacobsen, Mogens Havsteen; Buchardt, Ole; Engdahl, Tom; Holm, Arne
Tetrahedron Letters, 1991 , vol. 32, # 43 p. 6199 - 6202
反应条件
in dichloromethane 1 h; Ambient temperature;
参考文献
Leggio, Antonella; Liguori, Angelo; Procopio, Antonio; Sindona, Giovanni
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 13 p. 1969 - 1971
反应条件
1: 92 percent / CH2Cl2 / 1 h / Ambient temperature 2: 50 percent / silver benzoate / dioxane; H2O / 70 °C View Scheme
参考文献
Leggio, Antonella; Liguori, Angelo; Procopio, Antonio; Sindona, Giovanni
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 13 p. 1969 - 1971
反应条件
1: zinc / tetrahydrofuran / 20 °C 2: water; calcium chloride; sodium hydroxide / isopropyl alcohol View Scheme
参考文献
Ramesh; Raju; Srinivas; Sureshbabu; Vishwanatha; Hemantha
Rapid Communications in Mass Spectrometry, 2011 , vol. 25, # 14 p. 1949 - 1958