(2S,3R,4E)-2-叠氮-4-十八碳烯-1,3-二醇合成路线 （共 62 条）
反应条件
1: 90 percent / NaN3 / dimethylformamide / 36 h / 100 °C 2: 98 percent / NaOMe / methanol / 2 h / Ambient temperature View Scheme
参考文献
Synthesis, , # 1 p. 33 - 35
反应条件
1: 87 percent / DDQ, H2O / CH2Cl2 / 2 h / 0 °C 2: 94 percent / Bu4NF*3H2O / tetrahydrofuran / 1 h View Scheme
参考文献
Tetrahedron, , vol. 49, # 30 p. 6645 - 6650
反应条件
1: p-TsA / CH2Cl2 2: CH2Cl2 3: 80 percent / NaN3 / dimethylformamide 4: 3N HCl / tetrahydrofuran View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 7 p. 1191 - 1194
反应条件
1: CH2Cl2 2: 80 percent / NaN3 / dimethylformamide 3: 3N HCl / tetrahydrofuran View Scheme
参考文献
Tetrahedron Letters, , vol. 34, # 7 p. 1191 - 1194
反应条件
1: sodium azide / dimethylformamide / -20 °C 2: H2O; acetic acid / 45 °C View Scheme
参考文献
Carbohydrate Research, , vol. 158, p. 101 - 112
反应条件
1: diphenyldisulfide / cyclohexane; dioxane / 3 h / Irradiation 2: 99.4 percent / triethylamine / CH2Cl2 / 1.5 h / Ambient temperature 3: 57 percent / sodium azide / dimethylformamide / 3 h / 90 °C 4: 72 percent / 1 N hydrochloric acid / tetrahydrofuran / 1 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 45, # 9 p. 2557 - 2570
反应条件
1: LiBr 2: pyridine 3: NaN3 / dimethylformamide / Ambient temperature 4: HCl View Scheme
参考文献
Tetrahedron Letters, , vol. 27, # 4 p. 481 - 484
反应条件
hydrogen sulfide in pyridine; water 48 h; Ambient temperature;
参考文献
Duclos Jr., Richard I
Chemistry and Physics of Lipids, 2001 , vol. 111, # 2 p. 111 - 138
反应条件
in pyridine T=-10°C; 6 h;
参考文献
Liebigs Annalen der Chemie, , p. 663 - 668
反应条件
1: Zn; NH4Cl / methanol / 12 h / 20 °C View Scheme
参考文献
Kiso, Makoto; Nakamura, Akemi; Tomita, Yoshimi; Hasegawa, Akira
Carbohydrate Research, 1986 , vol. 158, p. 101 - 112
